Abstract
We have developed a new automatic sample-preparation robot system with use of the volumetric-weighing method. In this system, slurries, aqueous solutions, and other wet reagents are employed as starting materials and 64 (8×8) samples at the maximum are prepared on a library plate of 35 mm × 35 mm size. Volumetric-weighing and mixing of the starting materials and distributing reaction mixtures to the library plate are automatically performed by computer-controlled mechanisms with an easy-to-use programming software interface. While this robot is designed in terms of space saving and portability, it is able to equip with an atmosphere-controlled furnace to sinter the samples on the library plate. Typical preparation time for a library plate of 36 (6×6) samples is less than 40 min. This robot system is promising in enhancing throughput of wet-chemically synthesized materials researches.
Original language | English |
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Pages (from-to) | 2456-2460 |
Number of pages | 5 |
Journal | Applied Surface Science |
Volume | 252 |
Issue number | 7 |
DOIs | |
Publication status | Published - 21 Jan 2006 |
Event | Proceedings of the Third Japan-US Workshop on Combinatorial Material Science and Technology CMST-e SI - Duration: 7 Dec 2004 → 10 Dec 2004 |
Keywords
- Aqueous
- Combinatorial
- Robot
- Slurry
- Solution