A combinatorial sample-preparation robot system using the volumetric-weighing method

S. Suehara, T. Konishi, K. Fujimoto, T. Takeda, M. Fukuda, M. Koike, S. Inoue, M. Watanabe

Research output: Contribution to journalConference articlepeer-review

6 Citations (Scopus)

Abstract

We have developed a new automatic sample-preparation robot system with use of the volumetric-weighing method. In this system, slurries, aqueous solutions, and other wet reagents are employed as starting materials and 64 (8×8) samples at the maximum are prepared on a library plate of 35 mm × 35 mm size. Volumetric-weighing and mixing of the starting materials and distributing reaction mixtures to the library plate are automatically performed by computer-controlled mechanisms with an easy-to-use programming software interface. While this robot is designed in terms of space saving and portability, it is able to equip with an atmosphere-controlled furnace to sinter the samples on the library plate. Typical preparation time for a library plate of 36 (6×6) samples is less than 40 min. This robot system is promising in enhancing throughput of wet-chemically synthesized materials researches.

Original languageEnglish
Pages (from-to)2456-2460
Number of pages5
JournalApplied Surface Science
Volume252
Issue number7
DOIs
Publication statusPublished - 21 Jan 2006
EventProceedings of the Third Japan-US Workshop on Combinatorial Material Science and Technology CMST-e SI -
Duration: 7 Dec 200410 Dec 2004

Keywords

  • Aqueous
  • Combinatorial
  • Robot
  • Slurry
  • Solution

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